Heidolph Synthesis 1 Mode D'emploi page 56

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Thank you for buying a HEIDOLPH product. This appliance has been designed and
tested in compliance with DIN EN ISO 61010. It features ease of handling and long
service life.
SUMMARY ............................................................................................................... 56
STANDARD EQUIPMENT AND OPTIONS ............................................................. 58
GENERAL INFORMATION...................................................................................... 60
SAFETY INFORMATION ......................................................................................... 61
SET UP..................................................................................................................... 62
1. Liquid-Phase Synthesis ................................................................................. 62
1.1
1.1.1
1.1.2
1.1.3
1.1.4
1.1.5
1.2
1.2.1
1.2.2
1.3
1.3.1
1.3.2
1.3.3
1.4
2. Solid-phase synthesis .................................................................................... 71
2.1
2.1.1
2.1.2
2.1.3
2.1.4
2.1.5
2.1.6
2.1.7
2.2
2.2.1
2.3
2.4
2.4.1
2.4.2
2.5
2.5.1
2.5.2
2.6
3. Coolant fitting, liquid- or solid-phase synthesis .............................................. 80
3.1
3.2
4. Multiple-Evaporator........................................................................................ 80
Reaction Vessels ................................................................................ 62
Setup................................................................................................... 62
Install head.......................................................................................... 63
Built-in rotary valve.............................................................................. 63
Septa................................................................................................... 64
Capacity of reaction vessels................................................................ 64
Locate reaction vessels in heating- and condensation block .............. 64
Remove and install reaction vessels ................................................... 64
Vacuum-/ protective gas fitting with distributor (plenum)..................... 67
Connect vacuum- / inert gas lines ....................................................... 69
Connect vacuum- / inert gas lines ....................................................... 69
3-way valve, vacuum- / inert gas (standard equipment)...................... 69
Valve settings, vacuum-/ inert gas ...................................................... 70
Less reaction vessels .......................................................................... 70
Reaction vessels ................................................................................. 71
Setup:.................................................................................................. 71
Install and disassemble head / base ................................................... 72
Base with built-in filter ......................................................................... 72
Septa.................................................................................................. 72
Tube fitting, head and base................................................................ 73
Open and close valve of reaction vessel ............................................. 73
Capacity of reaction vessels................................................................ 74
Locate reaction vessels in heating- and condensation block .............. 74
Install vessels...................................................................................... 74
Connect vacuum / inert gas with vessels / plenum.............................. 75
Connect vacuum- / inert gas to plenum ports...................................... 75
3-way valve, vacuum-/ inert gas (standard equipment)....................... 76
Valve settings, vacuum- / inert gas ..................................................... 76
Connect waste cube, solid-phase synthesis........................................ 77
Convert waste cube for deviating number of vessels .......................... 78
Schematic, arrangement of waste cube tubes .................................... 79
Less reaction vessels .......................................................................... 79
Coolant connector, condensation zone ............................................... 80
Coolant fitting, conditioning zone for reactions
below room temperature...................................................................... 80
SUMMARY
56