Shimadzu LCMS-8045 CL Manuel D'instructions page 142

3 Préparation
### Sample Information ###
Sample Type:
### Tuning Condition ###
Detector Adjustment:
Resolution Adjustment:
FWHM of Spectrum:
Sensitivity Adjustment:
Mass Calibration:
### Tuning Result ###
Model:
Interface:
Polarity:
Tuning Mode:
Tuning Date:
Acquisition Mode:
Nebulizing Gas Flow:
Drying Gas Flow:
### Tuning Profile ###
CD:-10.00 kV
Int.: 236412
FWHM: 0.74
m/z : 45.05
Pre m/z: 388.25
Mag.: 83
Scan Range: 2.00 - 438.25 Scan Speed: 30 u/s Base Peak: 371.20 (1042664) Pre m/z: 388.25
100
45.05 89.05 133.10 177.10
m/z(Target)
388.25 > 45.05
388.25 > 89.05
388.25 > 133.10
388.25 > 177.10
DL Bias
Qarray Bias
Qarray RF
Multipole RF
Multipole1 Bias
Multipole1 Lens
Multipole2 Bias
Multipole2 Lens
Q1 Bias
CC Lens1
CC Lens2
CC Lens3
CC RF
CE
Q3 Bias
Q1 Pre Bias
Q3 Pre Bias
98
LCMS-8045 LCMS-8050
CL
PEG+PPG+Raffinose
On
On
0.70
On
On
LCMS-8045
DUIS
Pos
Auto
5/17/2017 11:13:39 AM
Product Scan
1.50(settings : 1.50) L/min
0.00(settings : 10.00) L/min
CD:-10.00 kV CD:-10.00 kV CD:-10.00 kV
Int.: 210232 Int.: 284641
FWHM: 0.73 FWHM: 0.70
m/z : 89.05 m/z : 133.10
Pre m/z: 388.25 Pre m/z: 388.25
Mag.: 92 Mag.: 68
100 200 300
m/z(Actual) Difference Width
45.05 0.00 0.74
89.05 0.00 0.73
133.10 0.00 0.70
177.10 0.00 0.69
Const 65.05 168.10 256.15
Const +0.0 +0.0 +0.0
Const +0.0 +0.0 +0.0
Scan +50.0 +19.3 +50.0
Scan +100.0 +30.0 +50.0
Const +0.0 +0.0 +0.0
Const -0.8 -0.8 -0.8
Const -0.8 -0.8 -0.8
Const -1.0 -1.0 -1.0
Const -3.5 -3.5 -3.5
Const +0.0 +0.0 +0.0
Const -100.0 -100.0 -100.0
Const -20.0 -20.0 -20.0
Const 45.05 89.05 133.10
Scan +100.0 +100.0 +120.0 +300.0
Scan -20.0 -25.0 -15.0
Scan -7.0 -7.0 -7.0
Const 107.15 1071.50 1893.40
Scan -15.0 -5.0 -50.0
Scan -15.0 -5.0 -50.0
CL
CID Gas Flow:
Heating Gas Flow:
Interface Bias:
Interface Current:
Interface Temp.:
DL Temp.:
Heat Block Temp.:
Q1 RF Gain:
Q1 RF Offset:
Q3 RF Gain:
Q3 RF Offset:
Q1 Post-rod Bias:
CID CELL Exit Lens:
Conversion Dynode:
Detector:
PG Vacuum:
IG Vacuum:
Corona Needle Voltage:
Corona Needle Current:
Int.: 167521
FWHM: 0.69
m/z : 177.10
Pre m/z: 388.25
Mag.: 115
400 500 600
Intensity
236412
210232
284641
167521
344.20 652.40 1004.60 1893.40
+0.0 +0.0 +0.0 +0.0
+0.0 +0.0 +0.0 +0.0
+90.0 +90.0 +130.0 +130.0 +130.0
+50.0 +50.0 +300.0 +300.0 +300.0
+0.0 +0.0 +0.0 +0.0
-0.8 -0.8 -0.8 -0.8
-0.8 -0.8 -0.8 -0.8
-1.0 -1.0 -1.0 -1.0
-3.5 -3.5 -3.5 -3.5
+0.0 +0.0 +0.0 +0.0
-100.0 -100.0 -100.0 -100.0 -100.0
-20.0 -20.0 -20.0 -20.0 -20.0
168.10 1893.40
+300.0 +300.0
-15.0 -15.0 -15.0
-7.0 -7.0 -9.0
-50.0
-50.0
230(settings : 230) kPa
5.02(settings : 5.00) L/Min
+4.00 kV
0.95 uA
100(settings : 100) C
249(settings : 250) C
399(settings : 400) C
4997
4970
4998
5002
-5.0 V
-1.7 V
-10.00 kV
-2.28(-2.28) kV
7.2e+001 Pa
2.1e-003 Pa
+4.50 kV
0.10 uA
700 800 900
+0.0
+0.0
+0.0
-0.8
-0.8
-1.0
-3.5
+0.0