Shimadzu LCMS-8045 CL Manuel D'instructions page 138

3 Préparation
Résultats du réglage automatique
### Sample Information ###
Sample Type:
### Tuning Condition ###
Detector Adjustment:
Resolution Adjustment:
FWHM of Spectrum:
Sensitivity Adjustment:
Mass Calibration:
### Tuning Result ###
Model:
Interface:
Polarity:
Tuning Mode:
Tuning Date:
Acquisition Mode:
Nebulizing Gas Flow:
Drying Gas Flow:
### Tuning Profile ###
CD:-10.00 kV
Int.: 2965936
FWHM: 0.63
m/z : 45.05
Mag.: 6
Scan Range: 2.00 - 2000.00 Scan Speed: 30 u/s Base Peak: 445.30 (20000000)
100
168.10
100
m/z(Target)
45.05
168.10
256.15
300.20
652.40
1004.60
1224.75
1603.15
DL Bias
Qarray Bias
Qarray RF
Multipole RF
Multipole1 Bias
Multipole1 Lens
Multipole2 Bias
Multipole2 Lens
Q1 Bias
CC Lens1
CC Lens2
CC Lens3
CC RF
CE
Q3 Bias
Q1 Pre Bias
Q3 Pre Bias
94
LCMS-8045 LCMS-8050
CL
PEG+PPG+Raffinose
On
On
0.70
On
On
LCMS-8045
DUIS
Pos
Auto
5/17/2017 10:56:35 AM
Q1 Scan(Use CID Gas)
1.50(settings : 1.50) L/min
0.00(settings : 10.00) L/min
CD:-10.00 kV CD:-10.00 kV
Int.: 2635370 Int.: 8448448
FWHM: 0.69 FWHM: 0.77
m/z : 168.10 m/z : 256.15
Mag.: 7 Mag.: 2
256.15
300.15
652.45
300 500 700
m/z(Actual) Difference Width
45.10 0.05 0.63
168.10 0.00 0.69
256.15 0.00 0.77
300.15 -0.05 0.78
652.45 0.05 0.75
1004.65 0.05 0.73
1224.80 0.05 0.74
1603.10 -0.05 (0.83)
Const 65.05 168.10
Const +0.0 +0.0 +0.0
Const +0.0 +0.0 +0.0
Scan +50.0 +19.3 +50.0
Scan +100.0 +30.0 +50.0
Const +0.0 +0.0 +0.0
Const -0.8 -0.8 -0.8
Const -0.8 -0.8 -0.8
Const -1.0 -1.0 -1.0
Const -3.5 -3.5 -3.5
Const +0.0 +0.0 +0.0
Const -100.0 -100.0 -100.0
Const -20.0 -20.0 -20.0
Const 65.05 168.10
Scan +200.0 +70.0 +110.0
Scan -15.0 -15.0 -15.0
Scan -15.0 -15.0 -15.0
Const 107.15 1071.50 1893.40
Scan -15.0 -5.0 -50.0
Scan -15.0 -5.0 -50.0
CL
LC/MS/MS Tuning
CID Gas Flow:
Heating Gas Flow:
Interface Bias:
Interface Current:
Interface Temp.:
DL Temp.:
Heat Block Temp.:
Q1 RF Gain:
Q1 RF Offset:
Q3 RF Gain:
Q3 RF Offset:
Q1 Post-rod Bias:
CID CELL Exit Lens:
Conversion Dynode:
Detector:
PG Vacuum:
IG Vacuum:
Corona Needle Voltage:
Corona Needle Current:
CD:-10.00 kV CD:-5.00 kV CD:-5.00 kV
Int.: 6576916 Int.: 4149214
FWHM: 0.78 FWHM: 0.75
m/z : 300.20 m/z : 652.40
Mag.: 2 Mag.: 4
828.55
1004.65
1224.80
900 1100
Intensity
2965936
2635370
8448448
6576916
4149214
6497677
2926660
444852
256.15 344.20 652.40 1004.60 1893.40
+0.0 +0.0 +0.0 +0.0
+0.0 +0.0 +0.0 +0.0
+90.0 +90.0 +130.0 +130.0 +130.0
+50.0 +50.0 +300.0 +300.0 +300.0
+0.0 +0.0 +0.0 +0.0
-0.8 -0.8 -0.8 -0.8
-0.8 -0.8 -0.8 -0.8
-1.0 -1.0 -1.0 -1.0
-3.5 -3.5 -3.5 -3.5
+0.0 +0.0 +0.0 +0.0
-100.0 -100.0 -100.0 -100.0
-20.0 -20.0 -20.0 -20.0
256.15 344.20 652.40 1004.60 1893.40
+130.0 +300.0 +300.0 +300.0 +300.0
-16.0 -17.0 -21.0 -25.0
-15.1 -15.2 -15.6 -16.0
-50.0
-50.0
229(settings : 230) kPa
5.01(settings : 5.00) L/Min
+4.00 kV
0.83 uA
99(settings : 100) C
250(settings : 250) C
400(settings : 400) C
4997
4970
---
---
-5.0 V
-4.0 V
-10.00 kV
-2.28(-2.28) kV
7.3e+001 Pa
2.1e-003 Pa
+4.50 kV
0.10 uA
CD:-10.00 kV CD:-10.00 kV
Int.: 6497677 Int.: 2926660
FWHM: 0.73 FWHM: 0.74
m/z : 1004.60 m/z : 1224.75
Mag.: 3 Mag.: 6
1312.80
1603.10
1300 1500 1700
+0.0
+0.0
+0.0
-0.8
-0.8
-1.0
-3.5
+0.0
-100.0
-20.0
-25.0
-17.0
Int.: 444852
FWHM: (0.83)
m/z : 1603.15
Mag.: 44
1893.30
1900