Shimadzu LCMS-8045 CL Manuel D'instructions page 140

3 Préparation
### Sample Information ###
Sample Type:
### Tuning Condition ###
Detector Adjustment:
Resolution Adjustment:
FWHM of Spectrum:
Sensitivity Adjustment:
Mass Calibration:
### Tuning Result ###
Model:
Interface:
Polarity:
Tuning Mode:
Tuning Date:
Acquisition Mode:
Nebulizing Gas Flow:
Drying Gas Flow:
### Tuning Profile ###
CD:-10.00 kV
Int.: 13933257
FWHM: 0.73
m/z : 45.05
Mag.: 1
Scan Range: 2.00 - 2000.00 Scan Speed: 30 u/s Base Peak: 445.35 (20000000)
100
168.10
100
m/z(Target)
45.05
168.10
256.15
300.20
652.40
1004.60
1224.75
1603.15
DL Bias
Qarray Bias
Qarray RF
Multipole RF
Multipole1 Bias
Multipole1 Lens
Multipole2 Bias
Multipole2 Lens
Q1 Bias
CC Lens1
CC Lens2
CC Lens3
CC RF
CE
Q3 Bias
Q1 Pre Bias
Q3 Pre Bias
96
LCMS-8045 LCMS-8050
CL
PEG+PPG+Raffinose
On
On
0.70
On
On
LCMS-8045
DUIS
Pos
Auto
5/17/2017 11:06:01 AM
Q3 Scan(Use CID Gas)
1.50(settings : 1.50) L/min
0.00(settings : 10.00) L/min
CD:-10.00 kV CD:-10.00 kV
Int.: 894757 Int.: 3389768
FWHM: 0.70 FWHM: 0.67
m/z : 168.10 m/z : 256.15
Mag.: 22 Mag.: 5
652.40
300.20
256.15
300 500 700
m/z(Actual) Difference Width
45.10 0.05 0.73
168.10 0.00 0.70
256.15 0.00 0.67
300.20 0.00 0.67
652.40 0.00 0.67
1004.60 0.00 0.68
1224.80 0.05 0.70
1603.25 0.10 0.70
Const 65.05 168.10
Const +0.0 +0.0 +0.0
Const +0.0 +0.0 +0.0
Scan +50.0 +19.3 +50.0
Scan +100.0 +30.0 +50.0
Const +0.0 +0.0 +0.0
Const -0.8 -0.8 -0.8
Const -0.8 -0.8 -0.8
Const -1.0 -1.0 -1.0
Const -3.5 -3.5 -3.5
Const +0.0 +0.0 +0.0
Const -100.0 -100.0 -100.0
Const -20.0 -20.0 -20.0
Const 65.05 168.10
Scan +200.0 +70.0 +110.0
Scan -5.0 -5.0 -5.0
Scan -7.0 -7.0 -7.0
Const 107.15 1071.50 1893.40
Scan -15.0 -5.0 -50.0
Scan -15.0 -5.0 -50.0
CL
CID Gas Flow:
Heating Gas Flow:
Interface Bias:
Interface Current:
Interface Temp.:
DL Temp.:
Heat Block Temp.:
Q1 RF Gain:
Q1 RF Offset:
Q3 RF Gain:
Q3 RF Offset:
Q1 Post-rod Bias:
CID CELL Exit Lens:
Conversion Dynode:
Detector:
PG Vacuum:
IG Vacuum:
Corona Needle Voltage:
Corona Needle Current:
CD:-10.00 kV CD:-5.00 kV CD:-5.00 kV
Int.: 5513393 Int.: 3729706
FWHM: 0.67 FWHM: 0.67
m/z : 300.20 m/z : 652.40
Mag.: 3 Mag.: 5
828.50
1004.60
1224.80 1312.80
900 1100
Intensity
13933257
894757
3389768
5513393
3729706
4922501
1949180
236558
256.15 344.20 652.40 1004.60 1893.40
+0.0 +0.0 +0.0 +0.0
+0.0 +0.0 +0.0 +0.0
+90.0 +90.0 +130.0 +130.0 +130.0
+50.0 +50.0 +300.0 +300.0 +300.0
+0.0 +0.0 +0.0 +0.0
-0.8 -0.8 -0.8 -0.8
-0.8 -0.8 -0.8 -0.8
-1.0 -1.0 -1.0 -1.0
-3.5 -3.5 -3.5 -3.5
+0.0 +0.0 +0.0 +0.0
-100.0 -100.0 -100.0 -100.0
-20.0 -20.0 -20.0 -20.0
256.15 344.20 652.40 1004.60 1893.40
+130.0 +300.0 +300.0 +300.0 +300.0
-5.0 -5.0 -5.0 -5.0
-7.1 -7.2 -7.6 -8.0
-50.0
-50.0
230(settings : 230) kPa
4.97(settings : 5.00) L/Min
+4.00 kV
0.90 uA
100(settings : 100) C
250(settings : 250) C
400(settings : 400) C
---
---
4998
5000
-5.0 V
-4.0 V
-10.00 kV
-2.28(-2.28) kV
7.2e+001 Pa
2.1e-003 Pa
+4.50 kV
0.10 uA
CD:-10.00 kV CD:-10.00 kV
Int.: 4922501 Int.: 1949180
FWHM: 0.68 FWHM: 0.70
m/z : 1004.60 m/z : 1224.75
Mag.: 4 Mag.: 10
1603.25
1300 1500 1700
+0.0
+0.0
+0.0
-0.8
-0.8
-1.0
-3.5
+0.0
-100.0
-20.0
-5.0
-9.0
Int.: 236558
FWHM: 0.70
m/z : 1603.15
Mag.: 83
1893.50
1900